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Getting Started Teledyne API – T101 Operation Manual
44
Table 3-9. NIST-SRM's Available for Traceability of H
2
S & SO
2
Calibration Gases
NIST-SRM
4
TYPE
NOMINAL
CONCENTRATION
2730
2731
Hydrogen sulfide in N
2
Hydrogen sulfide in N
2
5000 ppb
20 ppm
1693a
1694a
1661a
Sulfur dioxide in N
2
Sulfur dioxide in N
2
Sulfur dioxide in N
2
50 ppm
100 ppm
500 ppm
ZERO AIR
Zero air is similar in chemical composition to the earth’s atmosphere but without the gas
being measured by the analyzer, in this case H
2
S. If your analyzer is equipped with an
IZS or external zero air scrubber option, it is capable of creating zero air.
For analyzers without these options, a zero air generator such as the Teledyne API Model
701 can be used.
Once the appropriate pneumatic connections have been made, check all pneumatic fittings
for leaks using a procedure similar to that defined in Section 9.5.1.
07266B DCN6485
- MODEL T101 1
- UV FLUORESCENCE H 1
- S ANALYZER 1
- SAFETY MESSAGES 5
- CONSIGNES DE SÉCURITÉ 6
- WARRANTY 7
- ABOUT THIS MANUAL 9
- REVISION HISTORY 9
- 07266B DCN6485 10
- TABLE OF CONTENTS 11
- LIST OF APPENDICES 16
- LIST OF FIGURES 17
- LIST OF TABLES 18
- 1. INTRODUCTION 21
- 1.2. OPTIONS 22
- PARAMETER 25
- DESCRIPTION 25
- 2.2.1. SAFETY 26
- 2.2.2. EMC 26
- 3. GETTING STARTED 27
- 3.2. INSTRUMENT LAYOUT 28
- 3.2.2. REAR PANEL 32
- 3.3. ELECTRICAL CONNECTIONS 35
- ANALOG OUT 36
- 3.4. PNEUMATIC CONNECTIONS 41
- FL O W 44
- CO NTR O L 44
- Permeation Tube Heater 50
- INSTRUMENT CHASSIS 51
- VACUUM MANIFOLD 51
- 51
- NO 51
- CALIBRATION 52
- 3.5.4. FUNCTIONAL CHECK 54
- 3.6. INITIAL CALIBRATION 55
- 3.6.2. INTERFERENCES FOR H 58
- S MEASUREMENTS 58
- 4. OPERATING INSTRUCTIONS 59
- 4.2. SAMPLE MODE 60
- 4.2.2. WARNING MESSAGES 63
- 4.3. CALIBRATION MODE 64
- 4.4. SETUP MODE 66
- 4.4.4.7. Range Units 74
- 4.4.4.8. Dilution Ratio 75
- Table 4-6. Password Levels 76
- PRIMARY SETUP MENU 77
- SECONDARY SETUP MENU 78
- NO. VARIABLE DESCRIPTION 80
- ALLOWED 80
- See Section 6.8.1 81
- Press the PREV 82
- FUNCTIONS 83
- 4.6.1. SIGNAL I/O 85
- Table 4-12 88
- 4.6.3), then press: 93
- (Figure 4-5) 95
- 4.6.3.6. AIN Calibration 97
- 4.6.4. OPTIC TEST 99
- 4.6.5. ELECTRICAL TEST 100
- 4.6.6. LAMP CALIBRATION 101
- 4.6.7. PRESSURE CALIBRATION 102
- 4.6.8. FLOW CALIBRATION 103
- 4.6.9. TEST CHANNEL OUTPUT 104
- COMMUNICATION PORTS 105
- 4.7.4. RS-485 CONFIGURATION 109
- Contact your IT 113
- Network Administrator 113
- BUTTON FUNCTION 115
- >\ 115
- 4.7.7. USB CONFIGURATION 116
- RS-232 port 120
- 4.7.9. MODBUS SET UP 121
- ID DESCRIPTION 123
- 4.7.11. COM PORT BAUD RATE 125
- 4.7.12. COM PORT TESTING 126
- 4.8.1. DAS STRUCTURE 127
- 4.8.1.2. DAS Parameters 128
- 4.8.2. DEFAULT DAS CHANNELS 130
- LIST OF PARAMETERS 131
- LIST OF CHANNELS 131
- 0) CONC: ATIMER, 4, 800 133
- 4.8.2.3. Trigger Events 135
- Press SET> until… 136
- 4.8.2.6. Number of Records 139
- 4.8.2.8. Compact Report 141
- 4.8.2.9. Starting Date 141
- 4.8.2.11. HOLDOFF Feature 143
- 5. REMOTE OPERATION 145
- 5.1.1.2. Control Inputs 147
- 5.1.2.3. Command Syntax 150
- 5.1.2.4. Data Types 150
- 5.1.2.5. Status Reporting 151
- Parameter Standard Hessen 157
- Data Bits 8 7 157
- Stop Bits 1 2 157
- Parity None Even 157
- Duplex Full Half 157
- 6. CALIBRATION PROCEDURES 165
- 6.1.2. ZERO AIR 166
- 6.1.3. GAS STANDARDS 166
- 6.1.4. PERMEATION TUBES 166
- 6.2. MANUAL CALIBRATION 167
- Chassis 168
- STEP TWO: Set the expected H 169
- (At high 172
- span gas value: 173
- ZERO/SPAN VALVES 176
- No Valve Options Installed 180
- Table 6-2. AutoCal Modes 181
- 0.5 hours later each day 183
- Default 184
- REPORTING RANGE MODES 185
- MEASUREMENT MODE 186
- 6.10. CALIBRATION QUALITY 187
- 7. EPA PROTOCOL CALIBRATION 189
- TRACEABILITY 191
- 7.1.5. CALIBRATION FREQUENCY 192
- 7.1.6. RECORD KEEPING 192
- Table 7-3. Activity Matrix 193
- 7.3. ZERO AND SPAN CHECKS 195
- 7.4.1. PRECISION CALIBRATION 196
- 7.4.2. PRECISION CHECK 196
- 7.7. REFERENCES 198
- 8. INSTRUMENT MAINTENANCE 199
- 198 047400102 Rev XC 200
- 8.3. MAINTENANCE PROCEDURES 204
- 8.3.3. MAINTAINING THE SO 205
- SCRUBBER 205
- To check to see if your SO 206
- 8.3.5. MAINTAINING THE H 208
- CONVERTER 208
- 8.3.5.3. Changing the H 209
- 9.1. GENERAL TROUBLESHOOTING 213
- 9.1.4. STATUS LEDS 220
- Motherboard 221
- CPU Status LED 221
- 9.2. GAS FLOW PROBLEMS 222
- 9.3. CALIBRATION PROBLEMS 223
- 9.3.2. NO RESPONSE 224
- 9.3.6. NON-LINEAR RESPONSE 225
- 9.4.1. EXCESSIVE NOISE 226
- 9.4.2. SLOW RESPONSE 226
- 9.5. SUBSYSTEM CHECKOUT 227
- 9.5.4. DC POWER SUPPLY 229
- 9.5.8. RELAY BOARD 230
- 9.5.5. I 230
- 9.5.6. TOUCHSCREEN INTERFACE 230
- 9.5.7. LCD DISPLAY MODULE 230
- 9.5.9. MOTHERBOARD 231
- 9.5.10. CPU 232
- 9.5.11. RS-232 COMMUNICATION 233
- 9.5.12. PMT SENSOR 234
- 9.5.17. IZS OPTION 235
- 9.6. REPAIR PROCEDURES 236
- 9.6.3. REPLACING THE UV LAMP 239
- 9.8. TECHNICAL ASSISTANCE 243
- 10. PRINCIPLES OF OPERATION 245
- SO2OH2O3SH2 246
- SOaxexp1IIa 247
- = The rate at which the SO 248
- = Amount of excited state SO 248
- 10.2.1. UV SOURCE LAMP 249
- 10.2.3. THE PMT 250
- 10.2.4. OPTICAL FILTERS 251
- 10.2.5. OPTICAL LENSES 252
- 10.2.6.3. Dilution 254
- 10.2.6.5. Light Pollution 254
- 10.3. PNEUMATIC OPERATION 255
- 10.3.1. SAMPLE GAS FLOW 256
- SWITCHING 257
- 10.3.3. FLOW RATE CONTROL 257
- 10.3.6. SO 259
- 10.3.7. PNEUMATIC SENSORS 260
- CPU Card 261
- 10.4.1. CPU 263
- Figure 10-13. PMT Assembly 265
- 10.4.5. PMT COOLING SYSTEM 266
- 10.4.6. PMT PREAMPLIFIER 267
- PMT Preamp PCA 268
- 10.4.8.1. Heater Control 269
- 10.4.8.2. Valve Control 269
- 10.4.10.1. A to D Conversion 271
- 10.4.10.2. Sensor Inputs 271
- 10.4.11. ANALOG OUTPUTS 272
- 10.4.13. I 273
- C DATA BUS 273
- 10.4.14. POWER UP CIRCUIT 273
- 10.7.1. ADAPTIVE FILTER 276
- FEATURE 278
- 11.4.1. GENERAL RULES 282
- AND MAINTENANCE 284
- DO NOT use pink-poly bags 286
- GLOSSARY 287
- (Primary Setup Menu) 294
- ENTER SETUP PASS: 818 297
- GAS TYPE 299
- REPORTED 299
- Name Description 320
- Name Description Units 322
- MODBUS Coil Registers 326
- (single-bit; read/write) 326
- T101 Spare Parts List 329
- 07266B DCN6845 332
- Appendix C 333
- T101, M101E 333
- Auxiliary I/O Board (USB) 356
- Auxiliary I/O Board (ADC) 357
- GUI Interface 358
- Mode R32 R45 360
- Default A A 360
- MBUS B B 360
- From ICOP CPU 371
- To LCD Display 371
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